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Beilstein J. Org. Chem. 2017, 13, 855–862, doi:10.3762/bjoc.13.86
Graphical Abstract
Figure 1: Structures of kipukasins A–J.
Figure 2: Retrosynthetic analysis of kipukasin A.
Scheme 1: Synthesis of 2,4-dimethoxy-6-methylbenzoic chloride. Reagents and conditions: (a) POCl3, DMF, 0 °C ...
Scheme 2: Total synthesis of kipukasin A. Reagents and conditions: (a) I2, acetone, 0 °C to rt, 88%; (b) K2CO3...
Figure 3: X-ray structure of compound 13.
Beilstein J. Org. Chem. 2014, 10, 1681–1685, doi:10.3762/bjoc.10.176
Figure 1: Structures of trachycladine A and B.
Figure 2: Retrosynthetic analysis of trachycladines A and B.
Scheme 1: Synthesis of 5-deoxy-1-O-acetyl-2,3-di-O-benzoyl-2-C-β-methyl-D-ribofuranose (4). Reagents and cond...
Figure 3: The X-ray crystal structural of 1-O-methyl-3-O-(2,4-dichlorobenzyl)-5-deoxy-α-D-ribofuranose (9).
Scheme 2: Synthesis of trachycladine B (2). Reagents and conditions: (a) i. N,O-Bis(trimethylsilyl)acetamide ...
Scheme 3: Synthesis of trachycladine A (1). Reagents and conditions: (a) DBU, TMSOTf, CH3CN, 86%; (b) NH3 sat...